Laboratory Proficiency Program Series
AOCS offers more than 40 different series covering a wide array of testing skills and instrumentation. Participation counts towards ISO 17025 requirements. Successful completion of yearly series makes you eligible to apply for Approved Chemist status.
The AOCS Laboratory Proficiency Program (LPP) is the world's most extensive and respected collaborative proficiency testing program for oil- and fat-related commodities, oilseeds, oilseed meals, edible fats and plant proteins. More than 500 chemists participate to verify and demonstrate their lab's quality control.
Participants use AOCS or similar methods for sample analysis and then compare their results with a large cross-section of other laboratories using the same methods and samples.
View the program's A2LA Scope of Accreditation (.pdf).
LPP Award Winners:
Each year, AOCS publishes a list of LPP Award Winners to recognize the expertise of chemists in the program. The list consists of analysts who have scored in the top 10% of each series.
Program Details
Data submission and storage:
Participants log in and submit results on their personal dashboard, where they can also access their reports from the past five years.
Expert assistance available:
Each LPP series is supported by a committee of experts in the field who can answer questions related to testing method, results or both.
Comprehensive reports:
Participants receive quarterly reports that contain results of all participating labs (participant information is kept confidential) as well as a summary statistical analysis of their results including consensus mean and standard deviation, z-score (with chart) and a Kernel density plot. The AOCS Laboratory Proficiency program uses Robust Consensus Algorithm A from ISO 13528 and ISO 5725 Part 5 for the statistical analysis. After the 4th quarter, participants receive a proficiency report containing a performance evaluation for all participants for the entire LPP year.
To help participants understand the contents of their reports, Xin Wu, Technical Services Manager for AOCS, presented a walkthrough on how to interpret laboratory proficiency reports.
Enrollment:
There are four quarters in an AOCS LPP year, with the first quarter starting on July 1. Participants are free to enroll in any quarter. However, to be eligible for the AOCS Laboratory Proficiency Program Award, participants have to be enrolled for all four quarters in the same LPP year.
View the AOCS LPP Timeline (.pdf).
Sample preparation:
Some activities may be subcontracted.
To get started: Choose the series you need below and click on “Enroll Now.” Payment in full must be received prior to the payment deadline noted on the AOCS LPP Timeline (.pdf) to complete your enrollment.
Available Series
To renew: Log into your AOCS account to pay your proforma invoice in the “My Account” page.
Contact: If you need to make any changes to your proforma, or have any questions, please contact Sean Ekiss.
Sample(s) in this series
Corn Meal
Determination
Aflatoxins B1, B2, G1, and G2
Test Method
User-Specified Method
Sample(s) in this series
Cottonseed Meal
Determination
Aflatoxins B1, B2, G1, and G2
Test Method
User-Specified Method
Sample(s) in this series
Peanut Paste
Determination
Aflatoxins B1, B2, G1, and G2
Test Method
User-Specified Method
Sample(s) in this series
Pistachio and Almond
Determination
Aflatoxins B1, B2, G1, and G2
Test Method
User-Specified Method
Sample(s) in this series
Corn Meal
Determination
Total Aflatoxins
Test Method
Corn Meal Test Kit
Sample(s) in this series
Peanut Paste
Determination
Total Aflatoxins
Test Method
Peanut Paste Test Kit
Sample(s) in this series
1st quarter sample: Whole Egg Powder and Egg Yolk Powder
2nd quarter sample: Mixed Whole Egg, Egg Yolk Powder and Desiccated Cheese Powder
3rd quarter sample: Desiccated Powdered Turkey and Desiccated Powdered Chicken
4th quarter sample: Desiccated Powdered Beef and Desiccated Powdered Milk
Determination
Cholesterol
Test Method
AOAC 994.10
Sample(s) in this series
Corn Meal
Determination
Ash*
Crude Fat
Crude Fiber
Moisture
Protein
Test Method
User Specified
AOAC 920.39, 945.16 or 2003.06
AOAC 978.10 or Ba 6a-05 (filterbag)
NFTA 2.1.4 (105C/3 hr)
AOAC 990.03 (Combustion) or 2001.11 (Kjeldahl)
*Optional test
Sample(s) in this series
1st quarter samples: Margarine Oil and Vegetable Shortening
2nd quarter sample: Emulsified Shortening
3rd quarter sample: Vegetable Shortening
4th quarter samples: Emulsified Shortening and Vegetable Shortening
Determination
AOCS Color Red
Capillary Melting Point*
Free Fatty Acids
Iodine Value
Lovibond Color*
Mettler Dropping Point
α-Monoglycerides*
OSI*
Peroxide Value
Solid Fat Content
*Optional test
Sample(s) in this series
Corn Meal
Determination
B1*, B2*, B3*, and Total
Test Method
User-Specified Method
*Optional test
Sample(s) in this series
1st quarter samples: Palm Oil and Soybean Oil
2nd quarter samples: Vegetable Shortening and Cottonseed Oil
3rd quarter samples: Canola Oil and Coconut Oil
4th quarter samples: Sunflower Oil and Olive Oil
*Optional test
Sample(s) in this series
Marine Oil
Determination
Acid Value
p-Anisidine Value
EPA/DHA/Omega-3 Quantification
Peroxide Value
Totox Value
Sample(s) in this series
Marine Oil
Sample(s) in this series
October 1:
Coconut Oil – RBD
MCT Oil C8
Palm Kernel Oil – RBD
January 1:
Coconut Oil – RBD
MCT Oil 60/40 (Medium Chain Triglyceride)
MCT Oil
Determination
p-Anisidine Value
Fatty Acid Composition
Free Fatty Acids
Iodine Value
Moisture
Peroxide Value
Sample(s) in this series
1st quarter sample: Crude Coconut Oil
2nd quarter sample: RB Palm Oil
3rd quarter sample: Crude Safflower Oil
4th quarter sample: Crude Sunflower Oil
Determination
AOCS Color Red
Free Fatty Acids
Iodine Value
Mass/Unit Volume
Saponification Value
Sample(s) in this series
1st quarter samples: Whole Milk Powder and Infant Formula
2nd quarter samples: Dessert Ingredient I Chocolate Pudding/Beverage and Dessert Ingredient II Powdered Chocolate
3rd quarter samples: Cheese Powder and Egg Powder
4th quarter samples: Mayonnaise and Salad Dressing
Determination
Fatty Acid Composition
Minerals*
Total Fat
Total Protein
Vitamin A*
Vitamin D*
Vitamin E*
Test Method
Ce 1j-07
AOAC 985.35 or 984.27
User-Specified
User-Specified
AOAC 992.04 or 992.06
AOAC 992.26
AOAC 992.03
*Optional test
Sample(s) in this series
1st quarter samples: Soybean Meal and Canola Meal
2nd quarter samples: Peanut Meal and Soybean Meal
3rd quarter samples: Cottonseed Meal and Soybean Meal
4th quarter samples: Safflower Meal and Protein Concentrate
Determination
Crude Fiber
Moisture
Nitrogen
Oil (Petroleum Ether)
Sample(s) in this series
Olive Oil
PART A
Determination
Delta K (UV Extinction)
K270, K232, K225*
Free Fatty Acids
Peroxide Value
PART B
Determination
Diacylglycerols*
Fatty Acid Composition
Pyropheophytin*
Triglycerides (ECN 42)
PART C
Determination
Biophenols*
Contents of 2-Glycerol
Monopalmitate*
Sterenes*
Sterols
Stigmastadienes
Waxes
*Optional test
Sample(s) in this series
Olive Oil
Determination
Extra Virgin, Virgin & Lampante
Test Method
COI/T.20/Doc.15/Rev.11-2024
Sample(s) in this series
Palm Oil
Determination
Cloud Point*
Free Fatty Acids
Iodine Value
Lovibond Color
Slip Melting Point*
Solid Fat Content
*Optional test
Sample(s) in this series
1st quarter samples: Pinto Bean Powder and Black Bean Powder
2nd quarter samples: Red Bean Powder and Navy Bean Powder
3rd quarter samples: Chickpea Powder and Pinto Bean Powder
4th quarter samples: Yellow Pea Powder and Black Bean Powder
Determination
Crude Protein
Moisture and Volatile Matter
Ash
Fat
Crude Fiber
Dietary Fiber
Sample(s) in this series
1st quarter samples: Margarine Oil and Vegetable Shortening
2nd quarter sample: Emulsified Shortening
3rd quarter sample: Vegetable Shortening
4th quarter samples: Emulsified Shortening and Vegetable Shortening
Determination
Solid Fat Content
Test Method
Cd 16b-93
Sample(s) in this series
Soybean Oil
Determination
Free Fatty Acids
Lovibond Color*
Neutral Oil
*Optional test
Sample(s) in this series
1st quarter samples: Sesame Seed Oil, Avocado Oil
2nd quarter samples: Sunflower Oil, Chia Seed Oil
3rd quarter samples: Corn Oil, Canola Oil
4th quarter samples: Palm Oil, Rice Bran Oil
Determination
p-Anisidine Value
Fatty Acid Composition
Free Fatty Acids
Iodine Value
Moisture
Peroxide Value
Sample(s) in this series
Soybean Oil
Sample(s) in this series
Soy flour
Raw soybeans
Defatted soymeal
Soy protein concentrate
Soy protein isolate
Hulless barley
Pea flour
Pea protein concentrate
Determination
Trypsin Inhibitor Activity
Test Method
Ba 12a-2020
Sample(s) in this series
Vegetable Oil
Determination
AOCS Color Red
Lovibond Red Color*
*Optional test