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Methods by Subject

Section A: Vegetable Oil Source Materials

Aa 1-38 Sampling Cottonseed
Aa 10-88 Aflatoxin Standards
Aa 11-05 Aflatoxins by HPLC Using Postcolumn Photochemical Derivatization
Aa 2-38 Foreign Matter in Cottonseed Laboratory Sample
Aa 3-38 Moisture and Volatile Matter in Cottonseed
Aa 4-38 Oil Content, Crude in Cottonseed
Aa 5-38 SURPLUS Modified Kjeldahl Method (Cottonseed)
Aa 5-91 Nitrogen and Protein in Cottonseed and Cottonseed Meals, Modified Kjeldahl Method
Aa 6-38 Free Fatty Acids in Cottonseed
Aa 7-55 Residual Lint in Cottonseed
Aa 8-83 Aflatoxins in Cottonseed and Cottonseed Products, Thin-Layer Chromatography Method
Aa 9-86 Thin-Layer Chromatography Confirmation of Aflatoxins
Aa 9a-97 Aflatoxins in Corn and Peanuts by Thin-Layer Chromatography Method
Ab 1-49 Sampling Peanuts
Ab 2-49 Moisture and Volatile Matter in Peanuts
Ab 3-49 Oil in Peanuts
Ab 4-50 SURPLUS Modified Kjeldahl Method (Peanuts)
Ab 4-91 Nitrogen and Protein in Peanuts, Modified Kjeldahl Method
Ab 5-49 Free Fatty Acids in Peanuts
Ab 6-68 Aflatoxins in Peanuts and Peanut Products, Thin-Layer Chromatography Method
Ab 7-91 Aflatoxins in Peanuts and Peanut Products, HPLC Fluorescence Method
Ac 1-45 Sampling Soybeans
Ac 2-41 Moisture and Volatile Matter in Soybeans
Ac 3-44 Oil in Soybeans
Ac 4-41 SURPLUS Method Modified Kjeldahl Method (Soybeans)
Ac 4-91 Nitrogen and Protein in Soybeans, Modified Kjeldahl Method
Ac 5-41 Free Fatty Acids in Soybeans
Ac 6-16 Extraction and Indirect Enzyme-Linked-Lectin-Assay (ELLA) Analysis
Ad 1-48 Sampling Tung Fruit
Ad 2-52 Moisture and Volatile Matter in Tung Fruit and Hulls
Ad 3-52 Oil in Whole Tung Fruit
Ad 4-52 Physical Analysis of Tung Fruit
Ad 5-52 Oil in Tung Kernels
Ad 6-52 Oil in Hulled Tung Fruit
Ae 2-52 Moisture and Volatile Matter in Castor Seeds
Ae 3-52 Oil in Castor Seeds
Ae 4-52 Free Fatty Acids in Castor Seeds
Af 1-54 SURPLUS Sampling (Flaxseed)
Af 2-54 SURPLUS Moisture and Volatile Matter (Flaxseed)
Af 3-54 SURPLUS Oil Content (Flaxseed)
Ag 1-65 Oil in Safflower Seed
Ah 1-72 Aflatoxins in Copra and Copra Meal, Thin-Layer Chromatography Method
Ai 1-80 SURPLUS Sampling (Sunflower Seed)
Ai 2-75 Moisture and Volatile Matter in Sunflower Seed
Ai 3-75 SURPLUS Oil Content (Sunflower Seed)
Ai 4-75 SURPLUS Modified Kjeldahl Method (Sunflower)
Ai 4-91 Nitrogen and Protein in Sunflower Seed, Modified Kjeldahl Method
Aj 1-86 Aflatoxins in Corn, Minicolumn Method
Aj 2-86 Zearalenone and a-Zearalenol in Corn, HPLC Method
Aj 3-87 Aflatoxins in Corn, Thin-Layer Chromatography Method
Aj 4-89 Oil in Corn Germ
Aj 5-93 Fumonisins B1 and B2 in Corn and Corn-Based Food by Liquid Chromatography
Aj 5a-97 Fumonisins B1, B2, and B3 in Corn by Liquid Chromatography
Aj 6-95 Aflatoxins B1, B2, and G1 in Corn, Cottonseed, Peanuts, and Peanut Butter, ELISA Method
Aj 6a-97 Aflatoxins B1, B2, and G1 in Corn by ELISA Method
Ak 1-92 Glucosinolate Content in Rapeseed and Canola by HPLC
Ak 2-92 Chlorophyll Content in Rapeseed/Canola (Colza) by Spectrometry
Ak 3-94 Oil Content of Oilseeds by Nuclear Magnetic Resonance
Ak 4-95 Simultaneous Determination of Oil and Moisture Contents of Oilseeds Using Pulsed NMR Spectrometry
Ak 5-01 Simultaneous Determination of Oil and Moisture Contents of Oilseeds Residues Pulsed NMR Spectrometry
Am 1-92 Oil, Moisture and Volatile Matter, and Protein by Near-Infrared Reflectance
Am 1a-09 Near Infrared Spectroscopy Instrument Management and Prediction Model Development
Am 2-93 Oil Content in Oilseeds
Am 3-96 Oil in Oilseeds, Supercritical Fluid Extraction Method
Am 4-02 Impurities in Oilseeds
Am 5-04 Rapid Determination of Oil/Fat Utilizing High-Temperature Solvent Extraction

Section B: Oilseed Byproducts

Ba 1-38 Sampling of Oilseed By-Products
Ba 10-65 SURPLUS Protein Dispersibility Index (PDI)
Ba 10b-09 Protein Dispersibility Index (PDI)
Ba 11-65 Nitrogen Solubility Index (NSI)
Ba 12-75 Trypsin Inhibitor Activity
Ba 12a-20 Assaying Trypsin Inhibitor Activity
Ba 13-87 Free Hexane Content in Extracted Meals
Ba 14-87 Total Hexane Content in Extracted Meals
Ba 2a-38 Moisture and Volatile Matter Forced Draft Oven Method
Ba 2b-82 Moisture and Volatile Matter of Oilseed Protein Concentrates, Vacuum Oven Method
Ba 3-38 Oil in Seed Meals and Cakes
Ba 4a-38 SURPLUS Modified Kjeldahl Method (Oilseed Meals)
Ba 4b-87 SURPLUS Modified Kjeldahl Method (Copper Sulfate)
Ba 4c-87 SURPLUS Modified Kjeldahl Method (Kjel-Foss Automatic)
Ba 4d-90 Nitrogen and Protein Modified Kjeldahl Method
Ba 4e-93 Generic Combustion Method for Crude Protein
Ba 4f-00 Combustion Method for Crude Protein in Soybean Meal
Ba 5a-49 Ash in Oilseed Cake and Meals
Ba 5b-68 Acid-Insoluble Ash in Oilseed By-Products
Ba 6-84 Crude Fiber in Oilseed By-Products
Ba 6a-05 Crude Fiber in Feed by Filter Bag Technique
Ba 7-58 Free Gossypol in Cottonseed Products
Ba 7b-96 Free Gossypol in Cottonseed and Cottonseed By-Products, Rapid Method
Ba 8-78 Total Gossypol in Cottonseed By-Products
Ba 8a-99 Total Gossypol and Isomers in Cottonseed, Cottonseed By-Products by HPLC
Ba 9-58 Urease Activity
Bb 1-38 Sampling Cottonseed Linters and Cottonseed Hull Fibers
Bb 2-38 Oil in Cottonseed Hulls
Bb 3-47 Cellulose Yield Pressure-Cook Method
Bc 1-50 Sampling Soybean Flour
Bc 2-49 Moisture and Volatile Matter in Soybean Flour
Bc 3-49 Oil in Soybean Flour
Bc 4-49 SURPLUS Modified Kjeldahl Method (Soya Flour)
Bc 4-91 Nitrogen and Protein in Soybean and Canola Flours, Modified Kjeldahl Method
Bc 5-49 Ash in Soybean and Canola Flours
Bc 6-49 Crude Fiber in Soybean Flours
Bc 7-51 Screen Test for Soybean Flours
Bd 2-52 Moisture and Volatile Matter in Castor Pomace
Bd 3-52 Oil in Castor Pomace

Section C: Commercial Fats and Oils

C 1-47 Sampling of Commercial Fats and Oils
Ca 10-40 SURPLUS Break Test (Soybean Oil)
Ca 11-55 Ash in Fats and Oils
Ca 12-55 Phosphorus in Oils, Colorimetric
Ca 12a-02 Phosphorus in Oils,Colorimetric (ISO Method)nt in Fats and Oils
Ca 12b-92 Phosphorus by Direct Graphite Furnace Atomic Absorption Spectrometry
Ca 13-56 Total Gossypol in Crude Cottonseed Oil and Cottonseed Soap Stock, Spectrophotometric Method
Ca 14-56 Total, Free and Combined Glycerol Iodometric-Periodic Acid Method
Ca 14b-96 Free Glycerol in Selected Glycerides
Ca 15-75 Analyses for Chromium, Copper, Iron, and Nickel in Vegetable Oils
Ca 15b-87 Sodium and Calcium by Atomic Absorption Spectrophotometry
Ca 16-75 Polyethylene in Fats and Oils
Ca 17-01 Determination of Trace Elements in Oil by Inductively Coupled Plasma Optical Emission Spectroscopy
Ca 17a-18 Determination of Trace Elements in Oil by Inductively Coupled Plasma Optical Emission Spectroscopy
Ca 18-79 Chromium, Copper, Iron, Nickel, and Manganese in Triglyceride Oils by AAS Using a Graphite Furnace
Ca 18b-91 Copper, Iron, and Nickel by Graphite Furnace Atomic Absorption Spectrophotometry
Ca 18c-91 Lead by Direct Graphite Furnace Atomic Absorption Spectrophotometry
Ca 18d-01 Cadmium Content by Direct Graphite Furnace Atomic Absorption Spectrophotometry
Ca 19-86 Phospholipids in Vegetable Oils Nephelometric Method
Ca 20-99 Phosphorus in Oil by Inductively Coupled Plasma Optical Emission Spectroscopy
Ca 2a-45 Moisture in Fats and Oils, Distillation Method
Ca 2b-38 Moisture and Volatile Matter in Butter, Fats, Margarines, and Oils, Hot Plate Method
Ca 2c-25 Moisture and Volatile Matter, in Animal and Vegetable Fats, Air Oven Method
Ca 2d-25 Moisture and Volatile Matter, in Fats and Oils, Vacuum Oven Method
Ca 2e-84 Moisture Karl Fischer Reagent
Ca 2f-93 Moisture and Volatile Matter in Fats and Oils Modified Method
Ca 3a-46 Insoluble Impurities in Fats and Oils
Ca 3b-87 Hexane Residues in Fats and Oils
Ca 3c-01 Detection of a Volatile Organic Contaminant by GC-MS
Ca 3d-02 Sediment in Crude Fats and Oils, Centrifuge Method
Ca 3e-02 Visible Foots in Crude Fats and Oils
Ca 4-25 Soluble Mineral Matter and Fatty Acids Combined as Mineral Soap
Ca 5a-40 Free Fatty Acids in Crude and Refined Fats and Oils
Ca 5b-71 Crude Fatty Acids, Total Plus Saponifiable Matter
Ca 5c-87 SURPLUS Butyric Acid
Ca 5d-01 Free Fatty Acids in Crude Vegetable Oils by Capillary Gas Chromatography
Ca 5e-13 Butyric Acid, Capillary Column GLC Method
Ca 6a-40 Unsaponifiable Matter in Fats and Oils, Except Marine Oils
Ca 6b-53 Unsaponifiable Matter, High Level Method
Ca 6c-65 Hydrocarbons (Mineral Oil in Triglycerides) Oil)
Ca 7-35 SURPLUS Detection of Chlorinated Solvents (Beilstein Test)
Ca 8a-35 SURPLUS Detection of Sulfur (Coin Test)
Ca 8b-35 SURPLUS Detection of Sulfur (Silver Benzoate Test)
Ca 9a-52 Refining Loss
Ca 9f-57 Neutral Oil and Loss
Cb 1-25 Cottonseed Oil Presence, Halphen Test
Cb 2-40 Detection of Sesame Oil Modified Villavecchia Test
Cb 3-39 Detection of Teaseed Oil Fitelson Test (Modified Lieberman-Burchard Test)
Cb 4-35 Identification of Oils Crismer Test (Fryer and Weston Modification)
Cb 5-40 SURPLUS Detection of Foreign Fats Containing Tristearin in Pork Fats (Boemer Number)
Cb 6-86 Aflatoxins M1 and M2 in Dairy Products, TLC Method
Cc 1-25 Melting Point, Capillary Tube Method
Cc 10a-25 SURPLUS Specific Gravity of Oils and Liquid Fats
Cc 10b-25 Specific Gravity of Solid Fats and Waxes
Cc 10c-95 Determination of Mass per Unit Volume (Liter Weight) in Air of Oils and Fats
Cc 11-53 Cold Test for Fats and Oils
Cc 12-59 Titer Test
Cc 13a-43 Color of Fats and Oils, FAC Standards Comparison Methods
Cc 13b-45 Color Wesson Method Using Color Glasses Calibrated in Accordance with the Color Scale
Cc 13c-50 Color of Fats and Oils, Spectrophotometric Method
Cc 13d-55 Chlorophyll Pigments in Refined and Bleached Oils
Cc 13e-92 Color of Fats and Oil, Lovibond (ISO Method)
Cc 13f-94 Refined and Bleached Color and Saponification Color
Cc 13g-94 Saponification Color, High-Quality Tallows and Coconut Oils
Cc 13h-94 Saponification Color Tallows and Coconut Oils
Cc 13i-96 Determination of Chlorophyll Pigments in Crude Vegetable Oils
Cc 13j-97 Color of Fats and Oils, Automated Method
Cc 13k-13 Chlorophyll and Chlorophyll in Vegetable Oil, Spectrophotometric Determination
Cc 14-59 Congeal Point
Cc 15-60 SURPLUS Soap in Oil (Conductivity)
Cc 16-60 Consistency Penetrometer Method
Cc 17-95 Soap in Oil, Titrimetric Method
Cc 18-80 Mettler Dropping Point
Cc 2-38 SURPLUS Wiley Melting Point
Cc 3-25 Slip Melting Point, AOCS Standard Open Tube Melting Point
Cc 3b-92 Slip Melting Point, ISO Standard
Cc 4-25 SURPLUS Slipping Point (Soft Fats)
Cc 5-25 SURPLUS Flow Test
Cc 6-25 Cloud Point Test
Cc 7-25 Refractive Index of Fats and Oils
Cc 8a-52 Bleaching Test for Refined Cottonseed Oil
Cc 8b-52 Bleaching Test for Refined Soybean and Sunflower Oil
Cc 8d-55 Refined and Bleached Color in Tallow and Greases Intended for Soap Production
Cc 8e-63 Modified Bleach Test for Soybean Oil
Cc 8f-91 Evaluation of Bleaching Clays and Adsorbents
Cc 9a-48 Smoke, Flash and Fire Points, Cleveland Open Cup Method
Cc 9b-55 Flash Point, Closed Cup Method
Cc 9c-95 Determination of the Flashpoint by Pensky-Martens Closed Cup Flash Tester
Cd 1-25 SURPLUS Wijs Method for Iodine Value
Cd 10-57 SURPLUS Solid Fat Index (Dialometric)
Cd 11-57 SURPLUS a-Monoglycerides
Cd 11b-91 Mono- and Diglycerides by Capillary Gas Chromatography
Cd 11c-93 Monoglycerides, Diglycerides, and Triglycerides by Silica Gel Column Chromatography
Cd 11d-96 Mono- and Diglycerides HPLC-ELSD
Cd 12-57 SURPLUS Fat Stability, Active Oxygen Method
Cd 12b-92 Oil Stability Index
Cd 12c-16 Accelerated Oxidation Test for the Determination of Oxidation Stability
Cd 13-60 Hydroxyl Value of Fatty Oils and Alcohols
Cd 14-61 SURPLUS Isolated trans Isomers (FTIR)
Cd 14-95 Isolated trans Isomers, Infrared Spectrometric Method
Cd 14b-93 SURPLUS Fatty Acid Composition of Partially Hydrogenated Oils; A Combined GLC-IR Method
Cd 14c-94 SURPLUS trans Unsaturated Fatty Acids by Capillary Column Gas Chromatography
Cd 14d-99 Isolated trans Geometric Isomers in Fats and Oils by Attenuated Total Reflection Infrared Spectroscopy
Cd 14e-09 Total Isolated trans Fat by Negative Second Derivative Infrared Spectroscopic Method
Cd 14f-14 Rapid Determination of Total SFA, MUFA, PUFA, and trans Fatty Acid Content of Edible Fats and Oils by Pre-Calibrated FT-NIR
Cd 15-78 cis, cis Polyunsaturated Fatty Acids, Essential Fatty Acids (EFA)
Cd 16-81 Solid Fat Content (SFC) by Low-Resolution Nuclear Magnetic Resonance, Indirect Method
Cd 16-b-93 Solid Fat Content (SFC) by Low-Resolution Nuclear Magnetic Resonance, Direct Method
Cd 17-85 SURPLUS trans Unsaturation in Margarine by Gas Chromatography
Cd 18-90 p-Anisidine Value
Cd 19-90 2-Thiobarbituric Acid Value, Direct Method
Cd 1b-87 Iodine Value of Fats and Oils Cyclohexane Method
Cd 1c-85 Calculated Iodine Value
Cd 1d-92 Iodine Value of Fats and Oils, Cyclohexane-Acetic Acid Method
Cd 1e-01 Iodine Value by Pre-calibrated FT-NIR
Cd 2-38 SURPLUS Thiocyanogen Value
Cd 20-91 Polar Compounds in Frying Fats
Cd 21-91 Benzo(a)pyrene in Edible Oils and Fats
Cd 22-91 Polymerized Triglycerides by Gel-Permeation HPLC
Cd 23-93 Organophosphorus and Organochlorine Pesticide Residues from Edible Oils Using Multiple Solid Phase Extraction Cartridges
Cd 24-95 Dimethylpolysiloxanes in Fats and Oils
Cd 25-96 Heat Transfer Fluids in Oils—Dowtherm by GC
Cd 25a-00 Thermal Heating Fluids in Edible Oils and Oleochemicals—Dowtherm A by HPLC Coupled with Fluorescence Detector
Cd 25b-07 Thermal Heating Fluids in Vegetable Oils by GC
Cd 26-96 Stigmastadienes in Vegetable Oils
Cd 27-96 Steroidal Hydrocarbons in Vegetable Oils
Cd 28-10 Glycidyl Fatty Acid Esters in Edible Oils
Cd 29a-13 2- and 3-MCPD Fatty Acid Esters and Glycidol Fatty Acid Esters in Edible Oils and Fats by Acid Transesterification and GC/MS
Cd 29b-13 2- and 3-MCPD Fatty Acid Esters and Glycidol Fatty Acid Esters in Edible Oils and Fats by Alkaline Transesterification and GC/MS
Cd 29c-13 2- and 3-MCPD Fatty Acid Esters and Glycidol Fatty Acid Esters in Edible Oils and Fats by GC/MS (Difference Method)
Cd 29d-19 2-/3-MCPD Fatty Acid Esters and Glycidyl Fatty Acid Esters in Edible Oils and Fats by Enzymatic Hydrolysis
Cd 29e-19 2-/3-MCPD Fatty Acid Esters and Glycidyl Fatty Acid Esters in Fish Oils by Enzymatic Hydrolysis
Cd 29f-2021 2-/3-MCPD Fatty Acid Esters and Glycidyl Fatty Acid Esters in Edible Oils and Fats by Fast Alkaline Transesterification and GC-MS/MS
Cd 3-25 Saponification Value of Fats and Oils
Cd 30-15 Analysis of 2- and 3-MCPD Fatty Acid Esters and Glycidyl Fatty Acid Esters in Oil-Based Emulsions
Cd 3a-94 Saponification Value of Fats and Oils, by Calculation
Cd 3b-76 Saponification Value of Deodorizer Distillates and Sludges
Cd 3c-91 Saponification Value, Modified Method Using Methanol
Cd 3d-63 Acid Value of Fats and Oils
Cd 3e-02 Alkalinity in Fats and Oils
Cd 4-40 SURPLUS Acetyl and Hydroxyl Values
Cd 5-40 Reichert-Meissl, Polenske, and Kirschner Values, Modified AOAC Methods
Cd 6-38 SURPLUS Liquid and Solid Fatty Acids
Cd 7-58 Polyunsaturated Acids, Ultraviolet Spectrophotometric Method
Cd 8-53 SURPLUS Peroxide Value—Acetic Acid-Chloroform Method
Cd 8b-90 Peroxide Value, Acetic Acid, Isooctane Method
Cd 9-57 Oxirane Oxygen in Epoxidized Materials
Ce 1-62 SURPLUS Fatty Acid Composition by Gas Chromatography
Ce 10-02 Non-Cocoa Butter Vegetable Fats and Oils in Chocolate by the Analysis of Hydrocarbon Sterol Degradation Products
Ce 11-05 Cocoa Butter Equivalents in Cocoa Butter and Plain Chocolate
Ce 11a-07 Cocoa Butter Equivalents in Milk Chocolate
Ce 12-16 Sterols and Stanols in Food and Dietary Supplements Containing added Phytosterols
Ce 13-16 Determination of Cyclopropenoic and Nutritional Fatty Acids in Cottonseed and Cottonseed Oil by Gas Chromatography
Ce 1a-13 Fatty Acids in Edible Oils and Fats by Capillary GLC
Ce 1b-89 Fatty Acid Composition of Marine Oils by GLC
Ce 1c-89 SURPLUS Fatty Acid Composition by GLC, cis, cis and trans Isomers
Ce 1d-91 SURPLUS n-3 and n-6 Unsaturated Fatty Acids by Capillary GLC
Ce 1e-91 SURPLUS Fatty Acid Composition by Capillary GLC
Ce 1f-96 SURPLUS cis and trans Fatty Acids in Oils and Fats by Capillary GLC
Ce 1g-96 trans Fatty Acids by Silver-Ion Exchange HPLC
Ce 1h-05 Determination of cis-,trans-, Saturated, Monounsaturated and Polyunsaturated
Ce 1i-07 Saturated, cis-Monounsaturated, and cis-Polyunsaturated Fatty Acids
Ce 1j-07 cis-, trans-, Saturated, Monounsaturated, and Polyunsaturated Fatty Acids
Ce 1k-09 SURPLUS Fatty Acids by GC
Ce 2-66 Preparation of Methyl Esters of Fatty Acids
Ce 2b-11 Direct Methylation of Lipids in Foods by Alkali Hydrolysis
Ce 2c-11 Direct Methylation of Lipids in Foods by Acid-Alkali Hydrolysis
Ce 3-74 Tocopherols and Sterols in Soy Sludges and Residues by Gas-Liquid Chromatography
Ce 4-86 SURPLUS Erucic Acid by TLC
Ce 4-95 SURPLUS Erucic Acid by GLC
Ce 5-86 Triglycerides by Gas Chromatography
Ce 5b-89 Triglycerides in Vegetable Oils by HPLC
Ce 5c-93 Individual Triglycerides in Oils and Fats by HPLC
Ce 6-86 Antioxidants, Liquid Chromatographic Method
Ce 6a-2021 HPLC Analysis of Phenolic Antioxidants
Ce 7-87 Total Tocopherols in Deodorizer Distillate
Ce 8-89 Tocopherols and Tocotrienols in Vegetable Oils and Fats by HPLC
Ce 9-01 b-Carotene in Margarine-Carotene in Margarine
Cf 1-68 Analytical Guidelines for Testing Feed Grade Fat Products
Cg 1-83 Correlation of Oil Volatiles with Flavor Scores of Edible Oils
Cg 2-83 Flavor Panel Evaluation of Vegetable Oils
Cg 3-91 Analytical Guidelines for Assessing Oil Quality and Stability
Cg 4-94 Volatile Organic Compounds (VOC) in Fats and Oils by Gas Chromatography
Cg 5-97 Oven Storage Test for Accelerated Aging of Oils
Cg 6-01 Accelerated Light Exposure of Edible Vegetable Oils
Cg 7-05 Techniques for Assessing the Effects of Antioxidants in Oils and Fats
Ch 1-91 Preparation of Methyl Esters of Long-Chain Fatty Acids
Ch 2-91 Determination of Fatty Acids in Olive Oils by Capillary GLC
Ch 2a-94 trans Unsaturated Fatty Acids by Capillary Column Gas Chromatography
Ch 3-91 Fatty Acids in the 2-Position in the Triglycerides of Oils and Fats
Ch 3a-19 Determination of the Composition of Fatty Acids at the 2-Position of Oils and Fats-Enzymatic Transesterification Method using Candida antarctica Lipase
Ch 4-91 Chlorophyll Pigments in Olive Oils
Ch 5-91 Specific Extinction of Oils and Fats, Ultraviolet Absorption
Ch 6-91 Composition of the Sterol Fraction of Animal and Vegetable Oils and Fats by TLC and Capillary GLC
Ch 7-09 International Trade Standard Applying to Olive and Olive-Pomace Oils
Ch 8-02 Wax Content by Capillary Column Gas-Liquid Chromatography
Ci 1-91 Analytical Guidelines for Jojoba Oil Quality and Purity
Ci 2-91 Triglyceride Adulteration of Jojoba Oil
Ci 4-91 Acid Value of Jojoba Oil
Cj 1-94 DSC Melting Properties of Fats and Oils
Cj 2-95 X-Ray Diffraction Analysis of Fats
Cj 3-99 Calibration of Rheological Instruments
Cj 4-00 Spreadability
Ck 1-07 Analytical Guidelines for Assessing Feedstock to Ensure Biodiesel Quality
Ck 2-09 Determination of Various Properties of Biodiesel by the QTA® System Method
Ck 3-14 Analytical Guidelines for Assessing Corn Distillers Oil Quality

Section D: Soap and Synthetic Detergents

D 1-99 Comparison of AOCS and ASTM Methods for Soaps and Synthetic Detergent Analysis
Da 1-45 Sampling and Preparation of Laboratory Sample of Soap and Soap Products
Da 10-42 SURPLUS Unsaponified Plus Unsaponifiable Matter
Da 11-42 Unsaponifiable Matter in Soap and Soap Products
Da 12-48 Rosin in Soap and Soap Products, McNicoll Method
Da 13-48 Titer Test for Soap and Soap Products
Da 14-48 Acid Value of Fatty Acids
Da 15-48 Iodine Value, Soap and Soap Products, Wijs Method
Da 16-48 Saponification Value of Soap and Soap Products
Da 17-52 Borax in Soap and Soap Products
Da 18-48 Alkaline Silicates in Soap and Soap Products
Da 19a-42 Carbonates, Gravimetric Absorption Method
Da 19b-42 Carbonates, Volumetric Evolution Method
Da 20a-48 Phosphates in Soap and Soap Products, Gravimetric Method
Da 20b-57 Phosphates in Soap and Soap Products, Titrimetric Method
Da 21-48 Tetrasodium Pyrophosphate
Da 22-48 Sulfates in Soaps and Detergents, Gravimetric Method
Da 23-56 Free Glycerol Iodometric-Periodic Acid Method
Da 24-48 Sugars in Soap and Soap Products, Munson and Walker Method
Da 25-48 Starch in Soap and Soap Products, Munson and Walker Method
Da 26-42 Volatile Hydrocarbons in Soap and Soap Products
Da 27-48 Combined Sodium and Potassium Oxides in Soap and Soap Products
Da 28-39 Screen Test for Soap Powders
Da 2a-48 Moisture and Volatile Matter in Soap Moisture and Volatile Matte, Air Oven Method
Da 2b-42 Moisture in Soap and Soap Products, Distillation Method
Da 3-48 Alcohol-Soluble and Alcohol-Insoluble Matter in Soap and Soap Products
Da 31-58 Copper in Soap and Soap Products
Da 4a-48 Free Acid or Free Alkali in Soda Soap
Da 5-44 Free Alkali and Potassium Carbonate in Potash Paste Soaps
Da 6-48 Water-Insoluble Matter in Soap and Soap Products
Da 7-48 Total Alkalinity of Alcohol-Insoluble Matter in Soda Soap and Soda Soap Products
Da 8-48 Total Anhydrous Soap and Combined Alkali
Da 9-48 Chlorides in Soap and Soap Products
Db 1-48 Moisture and Volatile Matter in Soaps Containing Synthetic Detergents, Air Oven Method
Db 10-48 Fatty Matter in Soaps Containing Synthetic Detergents
Db 11-48 Rosin in Soaps Containing Synthetic Detergents, McNicoll Method
Db 2-48 Alcohol-Soluble and Alcohol-Insoluble Matter in Soap and Soap Products Containing Synthetic Detergents
Db 3-48 Free Acid or Free Alkali in Soap and Soap Products
Db 4-48 Water-Insoluble Matter in Soap and Soap Products
Db 5-48 Total Alkalinity of Alcohol-Insoluble Matter in Soda Soaps and Soda Soap Products Containing Synthetic Detergents
Db 6-48 Total Anhydrous Soap
Db 7-48 Chlorides in Soap and Soap Products Containing Synthetic Detergents, Indicator Method
Db 7b-55 Potentiometric Determination of Chlorides
Db 8-48 Saponification Value of Soap and Soap Products Containing Synthetic Detergents
Db 9-48 Alkaline Silicates in Soap Containing Synthetic Detergents
Dc 1-59 Sampling and Preparation of Laboratory Sample
Dc 2-59 Moisture in Fatty Alkyl Sulfate Products, Distillation Method
Dc 3a-59 Alcohol-Soluble Matter in Fatty Alkyl Sulfates
Dc 3b-59 Alcohol-Insoluble Matter of Fatty Alkyl Sulfates
Dc 4-59 Ester Sulfites in Fatty Alkyl Sulfates
Dc 5-59 Ester Sulfites in Fatty Alkyl Sulfates
Dc 6-59 Alkalinity or Acidity in Fatty Alkyl Sulfates
Dc 7-59 Sodium Sulfate in Fatty Alkyl Sulfates
Dc 8-59 Unsulfated Material in Fatty Alkyl Sulfates
Dd 1-59 Sampling and Preparation of Sample for Soap and Soap Products
Dd 2a-59 Moisture in Fatty Alkyl Sulfates, Distillation Method
Dd 2b-59 SURPLUS Modified Karl Fischer (Alkylbenzene Sulfonates)
Dd 3-60 Sodium Alkylbenzene Sulfonate by Ultraviolet Absorption
Dd 4-60 Neutral Oil (Unsulfonated Material) in Alkylbenzene Sulfonates
Dd 5-92 Sodium Linear Alkylbenzene Sulfonate (LAS) Color

Section T: Test Methods for Industrial Oils and Derivatives

Ta 1-09 Sampling of Industrial Oils and Derivatives
Ta 1e-70 Sampling of Dibasic Acids
Tb 1a-64 Moisture and Volatile Matter Fatty Acids, Hot Plate Method
Tb 2-64 SURPLUS Moisture, Modified Karl Fischer Reagent
Tb 2a-64 SURPLUS Modified Karl Fischer Method (Fatty Nitrogen Compounds)
Tc 1a-64 Nonvolatiles (Solids) Solutions of Drying Oils, Hot Plate Method
Tc 2a-64 Nonvolatiles (Solids) of Fatty Quaternary Ammonium Chlorides, Vacuum Oven Method
Td 1a-64 Color, Gardner 1963 (Glass Standards)
Td 1b-64 Platinum-Cobalt Scale for Light-Colored Liquids
Td 2a-64 Color, Photometric Index of Commerical Fatty Acids
Td 3a-64 Color Measurement by Color Stability for Fatty Acids, after Heating
Te 1a-64 Acid Value of Commercial Fatty Acids
Te 2a-64 Acid Value of Neutral and Synthetic Drying Oils, Epoxidized Oils, Fatty Alcohols, and Fatty Esters
Te 3a-64 Acid Value and Free Amine Value of Fatty Quaternary Ammonium Chlorides
Te 4a-70 Purity by Total Acidity and Acid Value, Dibasic Acids
Tf 1a-64 Total Amine Value of Fatty Amines, Potentiometric Method
Tf 1b-64 Total Amine Value of Fatty Amines, Indicator Method
Tf 2a-64 Primary, Secondary, and Tertiary Amine Values of Fatty Amines, Potentiometric Method
Tf 2b-64 Primary, Secondary, and Tertiary Amine Values of Fatty Amines, Indicator Method
Tf 3a-64 Percent Primary, Secondary, and Tertiary Amines in Fatty Amines
Tf 4a-77 Primary Amine Composition By Gas Chromatography
Tf 5-91 Composition of Dimer Acids by High- Performance Liquid Chromatography (HPLC)
Tg 1-64 Iodine Value, Wijs Method
Tg 1a-64 Iodine Value of Fatty Acids, Wijs Method
Tg 2a-64Iodine Value of Fatty Amines, Diamines, and Amidoamines, Modified Wijs Method
Tg 3a-64 Iodine Value of Fatty Quaternary Ammonium Chlorides, Modified Wijs Method
Th 1a-64 Diene Value of Drying Oils
Ti 1a-64 Spectrophotometric Determination of Conjugated Dienoic Acid in Dehydrated Castor Oils and Acids
Tj 1a-64 SURPLUS Polyunsaturated Acids, Ultraviolet Spectrophotometric Method
Tk 1a-64 Unsaponifiable Material in Drying Oils
Tl 1a-64 Saponification Value of Industrial Oils and Derivatives
Tm 1a-64 Ash in Drying Oils
Tm 2a-64 Ash of Fatty Quaternary Ammonium Chlorides
Tn 1a-64 Flash and Fire Points for Fatty Acids and Drying Oils, Cleveland Open Cup Method
Tn 2a-86 Flash Point of Fatty Quaternary Ammonium Chloride, Closed Cup Method
To 1a-64 Specific Gravity of Fatty Acids, Commercial
To 1b-64 Specific Gravity of Drying Oils
Tp 1a-64 Refractive Index of Drying Oils
Tq 1a-64 Viscosity of Transparent Liquids (Drying Oils) by Bubble Time Method
Tr 1a-64 Titer Test for Fatty Acids, Commercial
Ts 1a-64 Rosin Acids in Fatty Acids
Tt 1a-64 Acetone Tolerance of Heat-Bodied Drying Oils
Tu 1a-64 pH of Fatty Quaternary Ammonium Chlorides
Tv 1a-64 Average Molecular Weight of Fatty Quaternary Ammonium Chlorides
Tw 1a-64 Percent Non-Amines in Fatty Amines and Diamines
Tx 1a-66 Hydroxyl Value of Epoxidized Oils
Ty 1a-76 Dicarboxylic Acid Composition by Gas-Liquid Chromatography of Dimethyl Esters
Tz 1a-78 Activity of Hydrogenation Catalysts AOCS Recommended Practice
Tz 1b-79 Selectivity of Hydrogenation Catalysts

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